Research/Patents/US 4948766
US 4948766

RIGID MULLITE-WHISKER FELT AND METHOD OF PREPARATION

Assignee

NAVY, THE UNITED STATES OF AMERICA, AS REPRESENTED BY THE SECRETARY OF THE

Filed

Aug 5, 1988

Granted

Aug 14, 1990

Location

Arlington VA (defense contractors)

Abstract

A process in which (1) AlF3 and SiO2 or AlF3, SiO2, and Al2 O3 powders are formed into a green body of a desired shape and size; (2) the green body is heated at 700° C. to 950° C. in an anhydrous SiF4 atmosphere to form barlike topaz crystals; and then (3) heated in an anhydrous SiF4 atmosphere at about 1150° C. to 1700° C. to convert the barlike topaz crystals to needlelike single crystal mullite whiskers which form a porous, rigid felt structure. The felt has the same shape as the green body with about 1.5 or less percent change in linear dimensions. The felt can be used as preforms for ceramic-matrix or metal-matrix composites or by itself as thermal insulation.

Source: Google Patents

35 USC §181 Secrecy Order

Imposed

Oct 11, 1988

Rescinded

Jun 28, 1989

Duration

8 months

Inventor

  • 1INNA G. TALMY

Sensitive facility: Arlington VA (defense contractors)

Back to patent indexSource: USPTO 35 USC §181 secrecy order records